Precipitation behaviors of second-phase particles in grain-oriented electrical steels during manufacturing processes
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摘要: 利用場發射掃描電鏡觀察了以MnS為主要抑制劑的普通取向電工鋼加工過程中第二相粒子的分布狀態,統計了粒子面密度、平均尺寸以及相應的尺寸分布.結果顯示,熱軋加工造成了大量第二相粒子彌散、細小地析出,同時基體仍保持過飽和狀態.冷軋變形會造成第二相粒子的回溶行為,而基體的過飽和狀態會減弱回溶現象.中間退火與脫碳退火過程中會同時存在新粒子的形核及已析出粒子的粗化兩個過程,而在最終二次再結晶升溫階段則以第二相粒子明顯粗化為主.Abstract: The distribution of second phase particles in conventional grain-oriented electrical steels during manufacturing processes with MnS as inhibitors was observed by field emission scanning electron microscopy,while the areal particle density,the average particle size and the corresponding size distribution were statistically determined.It is indicated that hot rolling leads to dispersive precipitation of a large amount of fine second phase particles and the matrix keeps a supersaturated state further.Certain dissolution behaviors of second phase particles can be induced by cold rolling,in which the supersaturated state may reduce the dissolution.The precipitation nucleation of new particles and the coarsening of the particles coexist during the intermediate annealing and decarburizing annealing processes,after which the second-phase particles experience predominately the coarsening process during the final temperature rising stage of secondary recrystallization annealing.
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Key words:
- grain oriented electrical steel /
- second-phase particles /
- precipitation /
- inhibitors
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