由氨解法制備的Si<sub>3</sub>N<sub>4</sub>粉末的表面元素狀態

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由氨解法制備的Si₃N₄粉末的表面元素狀態

葛昌純, 夏元洛, 謝建剛, 黃向東, 丁宇, 張建偉

文章導航 > 工程科學學報 > 1991 > 13(S2): 1-6

葛昌純, 夏元洛, 謝建剛, 黃向東, 丁宇, 張建偉. 由氨解法制備的Si3N4粉末的表面元素狀態[J]. 工程科學學報, 1991, 13(S2): 1-6. doi: 10.13374/j.issn1001-053x.1991.s2.001

引用本文:

葛昌純, 夏元洛, 謝建剛, 黃向東, 丁宇, 張建偉. 由氨解法制備的Si₃N₄粉末的表面元素狀態[J]. 工程科學學報, 1991, 13(S2): 1-6. doi: 10.13374/j.issn1001-053x.1991.s2.001

Ge Changchun, Xia Yuanluo, Xie Jiangang, Huang Xiangdong, Ding Yu, Zhang Jianwei. Surface State of Fine Si3N4 Powders Made from Thermal Decomposition of SilicOn-Imide[J]. Chinese Journal of Engineering, 1991, 13(S2): 1-6. doi: 10.13374/j.issn1001-053x.1991.s2.001

Citation:

Ge Changchun, Xia Yuanluo, Xie Jiangang, Huang Xiangdong, Ding Yu, Zhang Jianwei. Surface State of Fine Si₃N₄ Powders Made from Thermal Decomposition of SilicOn-Imide[J]. Chinese Journal of Engineering, 1991, 13(S2): 1-6. doi: 10.13374/j.issn1001-053x.1991.s2.001

葛昌純, 夏元洛, 謝建剛, 黃向東, 丁宇, 張建偉. 由氨解法制備的Si3N4粉末的表面元素狀態[J]. 工程科學學報, 1991, 13(S2): 1-6. doi: 10.13374/j.issn1001-053x.1991.s2.001

引用本文:

葛昌純, 夏元洛, 謝建剛, 黃向東, 丁宇, 張建偉. 由氨解法制備的Si₃N₄粉末的表面元素狀態[J]. 工程科學學報, 1991, 13(S2): 1-6. doi: 10.13374/j.issn1001-053x.1991.s2.001

Ge Changchun, Xia Yuanluo, Xie Jiangang, Huang Xiangdong, Ding Yu, Zhang Jianwei. Surface State of Fine Si3N4 Powders Made from Thermal Decomposition of SilicOn-Imide[J]. Chinese Journal of Engineering, 1991, 13(S2): 1-6. doi: 10.13374/j.issn1001-053x.1991.s2.001

Citation:

Ge Changchun, Xia Yuanluo, Xie Jiangang, Huang Xiangdong, Ding Yu, Zhang Jianwei. Surface State of Fine Si₃N₄ Powders Made from Thermal Decomposition of SilicOn-Imide[J]. Chinese Journal of Engineering, 1991, 13(S2): 1-6. doi: 10.13374/j.issn1001-053x.1991.s2.001

由氨解法制備的Si₃N₄粉末的表面元素狀態

doi: 10.13374/j.issn1001-053x.1991.s2.001

特種陶瓷粉末冶金研究室

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- 文章訪問數: 274
- HTML全文瀏覽量: 71
- PDF下載量: 7
- 被引次數: 0
出版歷程
- 收稿日期: 1991-09-10
- 網絡出版日期: 2021-10-26

Surface State of Fine Si₃N₄ Powders Made from Thermal Decomposition of SilicOn-Imide

Laboratory of Special Ceramics and Powder Metallurgy

摘要: 用XPS表面分析,研究了由氨解法在不同溫度下熱解所得的Si₃N₄粉末,并與由硅粉氮化所得的商用Si₃N₄粉末作了比較。由氨解法制備的Si₃N₄粉末其表面存在兩種狀態的氧:結合狀態的氧和吸附態的氧,其表面組成為Si_2.2-2.7N_2.9-3.7O。由硅粉氮化所制得Si₃N₄其表面也存在兩種狀態的氧,其表面組成則為Si_0.8N_0.8O。
- 表面光電子能譜分析 /
- 氮化硅 /
- 粉末 /
- 熱分解
Abstract: Si₃N₄ powders made from imide process and thermal decomposed at different temperatures have investigated by XPS surface analysis; They were compared with a commercial Si₃N₄ powder made with nitridation process. Oxygen both in combined form of Si_2.2-2.7N_2.9-3.7O layer and absorbed form were found on the powder surface, in contrast to Si_0.8 N_0.8O layer and absorbed form in the case of Si₃N₄ powders made from Si aitridation.
- XPS /
- Si₃N₄ /
- powder /
- thermal decomposition

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文章訪問數: 274
HTML全文瀏覽量: 71
PDF下載量: 7
被引次數: 0

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