Preparation and Analysis of Titanium Di- and Trichlorides
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摘要: 本文用鈦還原四氯化鈦的方法研究了在KCl中,973K的溫度下制備低價鈦鹽的過程,可制得平均價低于2.5的低價鈦熔鹽。用改進后的量氫法,準確、簡便地分析了二價鈦和三價鈦的含量。Abstract: The paper studied the reactions for the formation of subhalides with average valence being less than 2.5 by the reaction of titanium with its liquid tetrachloride at lower temperature 973K in KCl melt.
An improved hydrogen evolution method has been developed to determine Ti2+ and Ti3+.-
Key words:
- low valent titanium chloride /
- analysis of titanium /
- disproportionation
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