The Formation of Cracks in a Nickel-base P/M Superalloy During Heat Treatment
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摘要: 業已證實,粉末高溫合金中原顆粒邊界(PPB)問題嚴重影響合金性能。本文研究了FGH95合金PPB對淬火裂紋的影響,通過對淬火開裂后樣品斷口形貌、析出相類型、表面俄歇譜化學成分分析找出淬火時裂紋形成的原因和控制因素。
實驗結果和分析表明;造成淬火裂紋形成的兩種機制,開裂嚴重的是由于PPB碳化物及在其外表面形成富氧層破壞合金的連續性,促使沿原顆粒邊界斷裂。開裂不嚴重的是由于γ相界析出大塊γ'相其周圍貧A1,Ti區形成易氧化層,促使沿γ相界斷裂。
基于兩種機制的提出,可以較好地說明影響淬火裂紋形成的主要原因是氧的污染和不適宜的淬火冷卻速度。Abstract: The effect of structural defects on the formation of quench cracks in a Nickel-base P/M superalloy was studied. The serious quench crack is due to the presence of rich-oxygen layer on the.Particle surface and the formation of PPB carbides destroying the continuity of the alloy and promoting fracture along the previous particle boundaries. The slight quench crack is due to the precipitation in a coarse form at the grain boundaries. The coarseγ' precipitates are surrounded by zones depleted Al,Ti froming oxide layers which promote the fracture path along the grain boundaries. The major reason of the formation of quench cracks is the contamination of oxygen in the early processing or unsuitable quench cooling rate during heat treatment. -

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